Summary report for Directory: home/perez/S-Gascoin

Report generated May 27, 2010; 09:32:38

Unit cell

a (Angstrom) 5.6298
b (Angstrom) 5.6286
c (Angstrom) 27.4543
alpha (°) 90.004
beta (°) 90.006
gamma (°) 120.013
Volume (A**3)753.3

Data collection

Summary

Total number of images collected431
Total exposure time13.4 hours
Data collection exposure time13.2 hours
Data collection wall-clock time13.8 hours

Experimental Conditions

Wavelength0.71073 A
Generator setting50kV 35mA
Crystal to detector distance34.00 mm

Scans

TypeName# imagesTotal
Rotation
Per frame
Rotation
Exposure
per frame
data collections01f193154.4° phi0.800°144 seconds
data collections02f127101.6° omega0.800°144 seconds
data collections03f103 82.4° phi0.800°14 seconds
Phi/Chii01f - i08f890 seconds

Eval Integration

Number of reflections  3948
Unique reflections  1172
Weak reflections   201
R-sym 0.074
R-meas 0.083

Bruker AXS Collect software