Summary report for Directory: home/data/crystallography/olivier/cr2392/long

Report generated Apr 15, 2009; 11:23:58

Unit cell

a (Angstrom)	17.364 +/- 0.002
b (Angstrom)	17.3766 +/- 0.0011
c (Angstrom)	6.9856 +/- 0.0006
alpha (°)	90.021 +/- 0.005
beta (°)	89.999 +/- 0.007
gamma (°)	119.979 +/- 0.005
Volume (A**3)	1825.75 +/- 0.19

Data collection

Summary

Total number of images collected	417
Total exposure time	11.9 hours
Data collection exposure time	11.8 hours
Data collection wall-clock time	12.4 hours

Experimental Conditions

Wavelength	0.71073 A
Generator setting	50kV 35mA
Crystal to detector distance	34.00 mm

Scans

Type	Name	# images	Total Rotation	Per frame Rotation	Exposure per frame
data collection	s01f	171	`136.8`° phi	0.800°	176 seconds
data collection	s02f	60	`48.0`° omega	0.800°	176 seconds
data collection	s03f	178	`142.4`° phi	0.800°	9 seconds
Phi/Chi	i01f - i08f	8			60 seconds

Eval Integration

Number of reflections	`24156`
Unique reflections	`16703`
Weak reflections	`5931`
Negative intensities	`77`
R-sym	`0.059`
R-meas	`0.079`

Bruker AXS Collect software